Extendingof the Life of Active Parts of Cold-Moulding Tools

After Slovakia’s accession to the EU, the opportunities for quality vacuum heat treatment of high alloy tool steels in heat treatment companies with precise direction and control of the upgrading process for the producers of the moulding tools have increased. Every year about one million tons of steel and 200 million tons of plastic are produced and processed. A big part of these materials is processed by moulding tools on which new and higher requirements are being placed: Accuracy, because of ever-increasing speeds of processing and loading there is a need to produce flawless details with ever tighter tolerances and thinner walls. Complete production on a single tool. Processing in dry and with minimal lubricating resulting in cost savings, reducing costs for cleaning of workpieces and machines and the reduction of environmental burden. Improved quality of product to minimise the need for additional work and the amount of scrap. This forces us to seek more efficient methods that help eliminate losses. One possibility is the coating of dies by a thin, hard and abrasion-resistant layer, which is specific for the particular type of loading tool [1, 2 and 3].


Introduction
After Slovakia's accession to the EU, the opportunities for quality vacuum heat treatment of high alloy tool steels in heat treatment companies with precise direction and control of the upgrading process for the producers of the moulding tools have increased. Every year about one million tons of steel and 200 million tons of plastic are produced and processed. A big part of these materials is processed by moulding tools on which new and higher requirements are being placed: -Accuracy, because of ever-increasing speeds of processing and loading there is a need to produce flawless details with ever tighter tolerances and thinner walls. -Complete production on a single tool. -Processing in dry and with minimal lubricating resulting in cost savings, reducing costs for cleaning of workpieces and machines and the reduction of environmental burden. -Improved quality of product to minimise the need for additional work and the amount of scrap. This forces us to seek more efficient methods that help eliminate losses. One possibility is the coating of dies by a thin, hard and abrasion-resistant layer, which is specific for the particular type of loading tool [1, 2 and 3].

Coatings and their properties
Processing technologies of depositions on surfaces of materials to improve their properties have been used for several decades. In the beginning, the chemical coating was used in the gas phase. This method is carried out under high temperature deposition (about 1000ºC), when the heat is affecting surface structure of the coated material, and therefore, its use is limited primarily on sintered carbides. The development of physical and plasma chemical methods done at about 500°C allowed coating of conventional tool steels [4 and 5].
The functionality of the temperature of the deposition and the deposition thickness, for certain methods of deposition is shown in Fig. 1. The depositions that are most used in practice for the improvement of the properties of the active part of the tools are shown in Table 1 and examples for productions are presented in Table 2.

Choice of the appropriate brand of the cold-moulding tool steel
Quality of the steel is given predominantly by the origin, the primary and secondary metallurgy or the subsequent treatment in the solid state (forming, annealing). For materials of the same brand, but supplied by two different producers and supply companies, differences in hardenability can attain more than 10%, in wear resistance of the order of tens of percent and as for toughness these differences may vary up to several times.
Cleanliness of metallurgical processes for the production of steel and finishing surfaces of tools or tool design can have a major impact on performance of tools. The technology of metallurgical processing of steel is graded according to the quality and purity of the final product, from conventional metallurgy to powder metallurgy [6, 7 and 8]. Examples of cold-moulding tool steel by various methods of metallurgical processing are given in Table 3.

Experimental part
We examined the effect of using of TiCN deposition coated PVD method onto a substrate -tool steel Vanadis 4, hardened The selected parameters of the depositions Table 1 Deposition

Hardness of the substrate
Hardness of the substrate was done by methodology Vickers HV60, in accordance with ISO 6507-1. Measurement results are presented in Table 7. The results represent the arithmetic average of three individual measurements.
Hardness of substrate Table 7 Marking of samples Hardeness HV60

Microhardness of the deposition
Measurement of microhardness of the deposition in accordance with ISO 6507-1 -both on the surface and the crosssectional view -could not be done due to the very small thickness of the coating, because there would be a complete penetration of the layer (from surface measurements), or overlapping of the measuring injection of the deposition to the substrate (measured in cross-section).
For this reason, it had to be done by the hardness measurement method known as "Nanoindentation" using the corresponding hardness testers CSM Instruments. All positions of performed measurements of microhardness of the depositon under nanoindentation were located in the working part of the samples. The measurement results are presented in Table 8. It

Chemical analysis of the substrate
Chemical analysis of the substrate was done by the method GDOES. The choice of the analytical method was based on the dimensional and geometric options of evaluated material. The results of chemical analysis of the substrate are shown in Table 4.
Results of chemical analysis of the substrate Table 4 Element The content of chemical elements (%)    secondary hardness 58-60HRC. Chemical analysis of deposition and the graphical representation of the percentage of the elements referred to in paragraph 4.2 and microhardness of the coating is shown in Table 8. With these modified components, we have reached 1.5 million strokes until the end of their operating life, which is a 20-fold increase in service life of active components of the tool.

Conclusion
We pointed out in the article that the appropriate choice of the coating method, layer and structure of the deposition for the mode of stress can significantly improve the properties of the active components of the cold-moulding tools, which is reflected in particular in a severalfold increase in durability of tools. The forming tools are characterized by the fact that their active components are usually produced of high alloy tool steels and their profile is complicated, with strict dimensional tolerances. PVD method has been successfully used in coating technology for this type of active components of cold-moulding tool because it retains all the desired properties. With DLC or PLC layers we are improving these properties. Currently mainly combinations of CVD and PVD or nanostructured coatings, which imply further improvement characteristics of cold-moulding tools, are gaining more and more importance.
represents the mean value of the 15 indentations, which have been done, and the variability of the results is the coefficient of variation of the series of results.
Hardness measuring of deposition -nanoindentation Table 8 Marking of samples

Experiment results
To produce the cutting punch and die we used the substrate -cold-moulding tool steel as the base material, known commonly as Vanadis 4 -the special tool steel produced by the method of PM from Uddeholm. Active parts were hardened and tempered to secondary hardness in vacuum hardening furnace. Chemical analysis of the substrate by the method GDOES is given in Table  4. The final hardness of the substrate is shown in Table 7.
In the first part of the experiment, we produced about 75 000 strokes with prepared active components without coating on the material CuNi25 of strength 90 HV30 until the end of life of the active parts. In the second part of the experiment, we used the active components using deposition of TiCN deposited by PVD on a substrate -the above-described tool steel hardened to